Chachula, S. T.; Hughes, R. P.; Glueck, D. S. Rhodium-Catalyzed Asymmetric Dehydrocoupling-Cyclophosphination of Supermesitylphosphines: Enantioselective Synthesis of a P-Stereogenic Benzophospholane via C–H Activation–Functionalization. Organometallics 2024, 43, 2797–2811.
Tipker, R. M.; Hughes, R. P.; Glueck, D. S.; Spinney, H. A.; Brammer, M. A.; Rheingold, A. L. Displacement of P-Stereogenic Phosphiranes from Rhodium by CO in Hydroformylation Catalysis. Organometallics 2024, 43, 427–431.
Garduño, J. A.; Sasser, A. J.; Sexton, H. J.; Hughes, R. P.; Glueck, D. S.; Rheingold, A. L. Diastereoselective and Reversible Metallacycle Formation by Attack of a Pt-PR2OH Group on a Coordinated Nitrile in Pt-Catalyzed Hydration. Organometallics 2024, 43, 381–394.
Tipker, R. M.; Muldoon, J. A.; Jo, J.; Connors, C. S.; Varga, B. R.; Hughes, R. P.; Glueck, D. S. Protonation of P-Stereogenic Phosphiranes: Phospholane Formation via Ring Opening and C–H Activation. ACS Omega 2023, 8, 12565-12572.
Chachula, S. T.; Scheetz, P. M.; Zureick, A. H.; Hughes, R. P.; Glueck, D. S.; Hernandez, R. E.; Figueroa, J. S.; Rheingold, A. L. Rhodium-Catalyzed Asymmetric Dehydrocoupling: Enantioselective Synthesis of a P-Stereogenic Diphospholane with Mistake-Correcting Diastereoselectivity. Organometallics 2023, 42, 1448–1453.
Garduño, J. A.; Glueck, D. S.; Hernandez, R. E.; Figueroa, J. S.; Rheingold, A. L. Protonolysis of the [B(ArF)4]− Anion Mediated by Nucleophile/Electrophile/Water Cooperativity in a Platinum–PMe2OH Complex. Organometallics 2022, 41, 1475–1479,
Glueck, D. S. Asymmetric Synthesis of P-Stereogenic Secondary Phosphine Oxides (SPOs). Synthesis 2022, 54, 271-280.
Tipker, R. M.; Muldoon, J. A.; Pham, D. H.; Varga, B. R.; Hughes, R. P.; Glueck, D. S.; Balaich, G. J.; Rheingold, A. L. Configurational Lability at Tetrahedral Phosphorus: syn/anti-Isomerization of a P-Stereogenic Phosphiranium Cation by Intramolecular Epimerization at Phosphorus. Angew. Chem. Int. Ed. 2022, 61, e202110753.
Glueck, D. S. Phosphiranes, Phosphirenes, and Heavier Analogues. In Comprehensive Heterocyclic Chemistry IV, Black, D. S.; Cossy, J.; Stevens, C. V., Eds. Elsevier: 2022; Vol. 1, pp 464-505.
Glueck, D. S. Intramolecular Attack on Coordinated Nitriles: Metallacycle Intermediates in Catalytic Hydration and Beyond. Dalton Trans. 2021, 50, 15953-15960.
Glueck, D. S. Catalytic Asymmetric Synthesis of P-Stereogenic Phosphines: Beyond Precious Metals. Synlett 2021, 32, 875-884.
Zimmerman, A. N.; Xu, R. S.; Reynolds, S. C.; Shipp, C. A.; Marshall, D. J.; Wang, G.; Blank, N. F.; Gibbons, S. K.; Hughes, R. P.; Glueck, D. S.; Balaich, G. J.; Rheingold, A. L. Diastereoselective Synthesis of P-Stereogenic Secondary Phosphine Oxides (SPOs) Bearing a Chiral Substituent by Ring Opening of (+)-Limonene Oxide with Primary Phosphido Nucleophiles. J. Org. Chem. 2020, 85, 14516–14526.
Scheetz, P. M.; Chachula, S. T.; Hughes, R. P.; Glueck, D. S.; Moore, C. E.; Gembicky, M.; Rheingold, A. L. Synthesis, Structure, Dynamics, and Enantioface-Selective η3-Benzyl Coordination in the Chiral Rhodium Complexes Rh(diphos*)(η3-CH2Ph). Organometallics 2020, 39, 3802–3816.
Glueck, D. S. Metal–Catalyzed P–C Bond Formation via P–H Oxidative Addition: Fundamentals and Recent Advances. J. Org. Chem. 2020, 85, 14276–14285.
Gibbons, S. K.; Valleau, C. R. D.; Peltier, J. L.; Cain, M. F.; Hughes, R. P.; Glueck, D. S.; Golen, J. A.; Rheingold, A. L. Diastereoselective Coordination of P-Stereogenic Secondary Phosphines in Copper(I) Chiral Bis(phosphine) Complexes: Structure, Dynamics, and Generation of Phosphido Complexes. Inorg. Chem. 2019, 58, 8854-8865.
Glueck, D. S. Modern Aspects of 31P NMR Spectroscopy. In Organophosphorus Chemistry: from Molecules to Applications; Iaroshenko, V., Ed.; Wiley-VCH: Weinheim, 2019, p 457-498.
Gibbons, S. K.; Xu, Z.; Hughes, R. P.; Glueck, D. S.; Rheingold, A. L. Chiral Bis(Phospholane) PCP Pincer Complexes: Synthesis, Structure, and Nickel-Catalyzed Asymmetric Phosphine Alkylation. Organometallics 2018, 37, 2159–2166.
Scheetz, P. M.; Blank, N. F.; Gibbons, S. K.; Glueck, D. S.; Rheingold, A. L. Oxidative Addition of Methylene Chloride to Me-DuPhos Complexes of Palladium and Rhodium. Inorg. Chim. Acta 2018, 483, 111-115.
Wang, G.; Gibbons, S. K.; Glueck, D. S.; Sibbald, C.; Fleming, J. T.; Higham, L. J.; Rheingold, A. L. Copper–Phosphido Intermediates in Cu(IPr)-Catalyzed Synthesis of 1-Phosphapyracenes via Tandem Alkylation/Arylation of Primary Phosphines. Organometallics 2018, 37, 1760–1772.
Deegan, M. M.; Muldoon, J. A.; Hughes, R. P.; Glueck, D. S.; Rheingold, A. L. Synthesis and Structure of Metal Complexes of P-Stereogenic Chiral Phosphiranes: An EDA-NOCV Analysis of the Donor–Acceptor Properties of Phosphirane Ligands. Organometallics 2018, 37, 1473–1482.
Muldoon, J. A.; Varga, B. R.; Deegan, M. M.; Chapp, T. W.; Eördögh, Á. M.; Hughes, R. P.; Glueck, D. S.; Moore, C. E.; Rheingold, A. L. Inversion of Configuration at the Phosphorus Nucleophile in Diastereoselective and Enantioselective Synthesis of P-Stereogenic syn-Phosphiranes from Chiral Epoxides. Angew. Chem. Int. Ed. 2018, 57, 5047–5051.
Glueck, D. S. 1,2-Bis((2S,5S)-2,5-dimethylphospholano)benzene (S,S)-Me-DuPhos and 1,2-Bis((2R,5R)-2,5-dimethylphospholano)benzene (R,R)-Me-DuPhos, First Update. In e-EROS Encyclopedia of Reagents for Organic Synthesis; John Wiley and Sons: 2018.
Scheetz, P. M.; Glueck, D. S.; Rheingold, A. L. Rhodium-Catalyzed Isomerization of a Bis(secondary phosphine) to an Unsymmetrical Diphosphine via P–C Cleavage and P–P and C–H Bond Formation. Organometallics 2017, 36, 3387–3397.
Gibbons, S. K.; Hughes, R. P.; Glueck, D. S.; Royappa, A. T.; Rheingold, A. L.; Arthur, R. B.; Nicholas, A. D.; Patterson, H. H. Synthesis, Structure, and Luminescence of Copper(I) Halide Complexes of Chiral Bis(phosphines). Inorg. Chem. 2017, 56, 12809–12820.
Anderson, B. J.; Reynolds, S. C.; Guino-o, M. A.; Xu, Z.; Glueck, D. S. Effect of Linker Length on Selectivity and Cooperative Reactivity in Platinum-Catalyzed Asymmetric Alkylation of Bis(phenylphosphino)alkanes. ACS Catal. 2016, 6, 8106–8114.
Wang, G.; Guino-o, M. A.; Glueck, D. S.; Golen, J. A.; Daley, C. J. A.; Rheingold, A. L. Synthesis of a Phosphapyracene via Metal-Mediated Cyclization: Structural and Reactivity Effects of Acenaphthene Precursors. Dalton Trans. 2015, 44, 9943–9954.
Emerson, E. W.; Cain, M. F.; Sanderson, M. D.; Knarr, C. B.; Glueck, D. S.; Ahern, J. C.; Patterson, H. H.; Rheingold, A. L. Synthesis, structure, and luminescence of the "octahedral" cluster Cu4I4(rac-IsMePCH2PMeIs)2 (Is = 2,4,6-(i-Pr)3C6H2). Inorg. Chim. Acta 2015, 427, 168-172.
Xu, Z.; Cain, M. F.; Rupert, A. V.; Glueck, D. S.; Golen, J. A.; Rheingold, A. L. Selective formation of a C3-symmetric P-stereogenic tris(phosphine) via platinum-catalyzed asymmetric alkylation of a tris(secondary phosphine). Tetrahedron: Asymmetry 2015, 26, 1459–1468.
Reynolds, S. C.; Hughes, R. P.; Glueck, D. S.; Rheingold, A. L. Org. Lett. 2012, 14, 4238–4241. Synthesis, Reactivity, and Resolution of a C2–Symmetric, P–Stereogenic Benzodiphosphetane, a Building Block for Chiral Bis(phosphines).
Guino-o, M. A.; Zureick, A. H.; Blank, N. F.; Anderson, B. J.; Chapp, T. W.; Kim, Y.; Glueck, D. S.; Rheingold, A. L. Organometallics 2012, 31, 6900-6910. Synthesis and Structure of Platinum Bis(phospholane) Complexes Pt(diphos*)(R)(X), Catalyst Precursors for Asymmetric Phosphine Alkylation.
Chapp, T. W.; Schoenfeld, A. J.; Sanderson, M. D.; Chang, C. L.; Glueck, D. S.; Golen, J. A.; Moore, C. E.; Rheingold, A. L. Organometallics 2012, 31, 5573–5585. Synthesis, Structure, Dynamics, and Selective Methylation of Platinum and Palladium Diphosphametallacyclobutane Complexes.
Cain, M. F.; Glueck, D. S.; Golen, J. A.; Rheingold, A. L. Organometallics 2012, 31, 775-778. Asymmetric Synthesis and Metal Complexes of a C3-Symmetric P-Stereogenic Triphosphine, (R)-MeSi(CH2PMe(t-Bu))3 (MT-Siliphos).
Zuzek, A. A.; Reynolds, S. C.; Glueck, D. S.; Golen, J. A.; Rheingold, A. L. Organometallics 2011, 30, 1812-1817. Synthesis and Structure of Gold and Platinum Menthyl Complexes.
Seibert, A. R.; Cain, M. F.; Glueck, D. S.; Nataro, C. J. Organomet. Chem.2011, 696, 2259-2262. Electrochemistry of P(CH2Fc)3 and derivatives.
Glueck, D. S. Catal. Sci. Technol. 2011, 1, 1099-1108. Selectivity via catalyst or substrate control in catalytic asymmetric transformations of bifunctional symmetrical substrates. (invited review)
Cain, M. F.; Reynolds, S. C.; Anderson, B. J.; Glueck, D. S.; Golen, J. A.; Moore, C. E.; Rheingold, A. L. Inorg. Chim. Acta 2011, 369, 55-61. Synthesis, Structure and Spectroscopic Properties of 2,3-bis(diphenylphosphino)quinoxaline (dppQx) and Its Copper(I) Complexes. (special R.G. Bergman issue)
Cain, M. F.; Hughes, R. P.; Glueck, D. S.; Golen, J. A.; Moore, C. E.; Rheingold, A. L. Inorg. Chem.2010, 49, 7650–7662. Synthesis and Structure of Intermediates in Copper-Catalyzed Alkylation of Diphenylphosphine. (cover picture)
Glueck, D. S. Top. Organomet. Chem.2010, 31, 65-100. Recent Advances in Metal-Catalyzed C–P Bond Formation. (invited review)
Lane, E. M.; Chapp, T. W.; Hughes, R. P.; Glueck, D. S.; Feland, B. C.; Bernard, G. M.; Wasylishen, R. E.; Rheingold, A. L. Inorg. Chem.2010, 49, 3950–3957. Synthesis of Gold Phosphido Complexes Derived from Bis(secondary) Phosphines. Structure of Tetrameric [Au(MesP(CH2)3PMes)Au]4.
Chapp, T. W.; Schoenfeld, A. J.; Glueck, D. S. Organometallics2010, 29, 2465-2473. Effects of Linker Length on the Rate and Selectivity of Platinum-Catalyzed Asymmetric Alkylation of the Bis(isitylphosphino)alkanes IsHP(CH2)nPHIs (Is = 2,4,6-(i-Pr)3C6H2, n = 1–5).
Chapp, T. W.; Glueck, D. S.; Golen, J. A.; Moore, C. E.; Rheingold, A. L. Organometallics2010, 29, 378-388. Platinum-Catalyzed Asymmetric Alkylation of Bis(isitylphosphino)ethane: Stereoselectivity Reversal in Successive Formation of Two P-C Bonds.
